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Adsorption behavior of water vapor in lignite pores: Experimentalstudy and molecular dynamics simulation

2024 No. 05
231
103
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Authors:
WANG Chengyong
XING Yaowen
WANG Shiwei
CHEN Peng
LI Jihui
GUI Xiahui
Unit:
School of Mining and Mechanical Engineering,Liupanshui Normal University
Chinese National Engineering ResearchCenter of Coal Preparation and Purification,China University of Mining and Technology
School of Chemical and EnvironmentalEngineering,China University of Mining and Technology,Beijing
Abstract:

Deeply understanding the adsorption of water on lignite is one of the theoretical foundations of lignite drying and upgrading technology. The oxygen-containing functional groups and pore structure of lignite were analyzed using Fourier Transform Infrared Spectroscopy(FTIR), Scanning Electron Microscopy (SEM), and low-temperature nitrogen adsorption/ desorption experiments. The adsorption behavior of water vapor in the pores of lignite was investigated using water vapor adsorption/ desorption experiments and Molecular Dynamics(MD) simulations. Results show that the rich oxygen-containing functional groups and numerous micropores and mesopores (with the poresize mainly around 2 nm) in lignite samples provide adsorption sites and places for water vapor. The adsorption process of water vapor onthe coal sample can be divided into three stages. In the first stage, with the relative vapor pressure (P/ P0)<0.21, water molecules directlyadsorbe on oxygen-containing functional groups, and the adsorption speed is the highest. In the second stage (P/ P0 = 0.21-<0.71),water molecules interact with adsorbed water molecules, promoting the gradual growth of water clusters. In the third stage (P/ P0≥0.71),water clusters fill the pores and the capillary condensation appeared, the adsorption speed in this stage is slightly higher than in the secondstage. According to the fitting results of the Dent model on the water vapor adsorption isotherm, the adsorption type belonged to multi-stage adsorption, including primary adsorption (first stage) and secondary adsorption (second and third stages). The primary adsorptionenergy (-48.77 kJ/ mol) is significantly greater than the liquefaction heat of water (EL = -43.99 kJ/ mol), while the secondary adsorptionenergy (-42.28 kJ/ mol) is only slightly less than EL, indicating that the water adsorbed on lignite is liquid. There is a significant desorption hysteresis phenomenon during the water vapor desorption process, indicating that the water vapor adsorbes stably and is difficult to remove. High pressure hysteresis occurr in the range of P/ P0 ≈0.4-0.9, mainly caused by capillary condensation and the " ink bottle"effect. Low pressure hysteresis occurr in the range of P/ P0<0.4, caused by strong interactions between water molecules and oxygen-containing functional groups. The MD simulation results are consistent with the analysis of water vapor adsorption/ desorption isotherm. Water molecules preferentially adsorb in the pore and form hydrogen bonds with oxygen-containing functional groups on the pore walls, with adiffusion coefficient (2.98×10-5 cm2 / s) similar to that of liquid water.

Keywords:
lignite
pore structure
oxygen-containing functional group
water vapor adsorption
Dent model
molecular dynamics simulation
Citation format:
王成勇(1987—),男,四川泸州人,副教授,博士研究生。E-mail:wangchengyong87@163.com
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Citation format:
WANG Chengyong,XING Yaowen,WANG Shiwei,et al.Adsorption behavior of water vapor in lignite pores: Experimentalstudy and molecular dynamics simulation[J].Clean Coal Technology,2024,30(5):162-171.

About Journal

  • Executive director

    China Coal Science and Industry Group Co., Ltd

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    Coal Science Research Institute Co., Ltd
    Coal Industry Clean Coal Engineering
    Technology Research Center

  • Editor in Chief

    XIE Qiang

  • Vice Editor-in-Chief

    YU Chang
    SHI Yixiang
    ZHAO Yongchun
    DUAN Linbo
    CAO Jingpei
    ZENG Jie

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