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Composition, structure and properties of low melting Fischer-Tropsch waxes

2023 No. 06
409
189
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Authors:
YU Yanan
CI Donghui
ZHANG Shengzhen
CHEN Shengli
ZHANG Wei
LI Hu
JIANG Chenguang
Unit:
National Institute of Clean-and-Low-Carbon Energy
College of Chemical Engineering and Environment,ChinaUniversity of Petroleum
CTL Company,China Energy NingXia Coal Industry Company
Abstract:

The composition, structure and properties of No.52 F-T wax and four kinds of No.52 petroleum wax were investigated by the use of Gas Chromatography (GC), X-ray diffraction (XRD), Differential Scanning Calorimetry (DSC)and other characterization methods. The results show that the five waxes are mainly composed of long-chain alkanes, and in compared with petroleum waxes, the F-T wax has narrow carbon number distribution, highn-alkane component content,high saybolt color value,low iso-alkane component content ,low needle penetrationvalue, and low oil content. At room temperature, both F-T and the petroleumwaxeshave the orthorhombic crystal structure. F-T wax has similar DSC as petroleum wax with respect to a weak solid-solid phase transition peak and a strong solid-liquid phase transition peak. According to the results of the polarized microscope, the oblique square sheet-shaped crystals are arranged closely. In the process of cooling, the radial size of the sheet wax crystal gradually increases, and the wax crystal will continue to form a large solid crystal group, thus forming a three-dimensional spatial network structure. It indicates the high content of n-alkanes in the wax of No.52, which is consistent with the GC results.The No.52 F-T wax is better than petroleum wax in terms of physical pr- operties and chemical composition, and is similar to petroleum wax with respect to crystal structure and thermal properties.The No.52 F-T wax can be used as petroleum wax. The low-toxicity special extraction agent developed by NICE can realize the production of No.48-54 fully refined paraffin wax in the aromatics-free system, which is expected to replace the traditional solvent.

Keywords:
Fischer-Tropsch waxes
low melting point
n-alkanes
crystal structure
solid-solid transition
Citation format:
于亚楠(1997—),女,河南洛阳人,硕士研究生。E-mail:1668084885@qq.com
通讯作者:张胜振(1976—),男,山东济宁人,高级工程师,博士。E-mail:shengzhen.zhang@chnenergy.com.cn
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Citation format:
YU Yanan,CI Donghui,ZHANG Shengzhen,et al.Composition, structure and properties of low melting Fischer-Tropsch waxes [J].Clean Coal Technology,2023,29(6):90-98.

About Journal

  • Executive director

    China Coal Science and Industry Group Co., Ltd

  • Sponsored by

    Coal Science Research Institute Co., Ltd
    Coal Industry Clean Coal Engineering
    Technology Research Center

  • Editor in Chief

    XIE Qiang

  • Vice Editor-in-Chief

    YU Chang
    SHI Yixiang
    ZHAO Yongchun
    DUAN Linbo
    CAO Jingpei
    ZENG Jie

  • Publication Frequencies

    Monthly

  • ISSN

    1006-6772

  • CN

    11-3676/TD

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  • CSTPCD
  • RCCSE(A+)
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