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Composition structure and properties of four narrow fraction Fisher-Tropsch waxes

2022 No. 02
428
199
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Authors:
XIE Haodong
YU Yanan
ZHANG Shengzhen
JIANG Chenguang
KANG Shanjiao
ZHANG Fan
CHEN Shengli
Unit:
College of Chemical Engineering and Environment,China University of Petroleum;National Institute of Clean-and-Low-Carbon Energy;College of Mechanical and Transportation Engineering,China University of Petroleum
Abstract:

The Fischer-Tropsch synthesis crude waxes,which were produced by indirect coal liquefaction demonstration units from China Energy Ningxia Coal,were separated into four narrow fraction waxes by solvent extraction coupled with fractional crystallization. The composition,structure and properties of the four narrow fraction waxes were investigated by Gas Chromatography (GC),Fourier Transform Infrared Spectroscopy (FT-IR),Differential Scanning Calorimetry (DSC),Thermogravimetric Analysis (TG) and other characterization methods. The results show that the four narrow fraction waxes are similar to each other in composition,with a normal distribution of carbon numbers and mainly composed of long-chain alkanes. With the increase of molecular weight of the narrow fraction waxes,their melting point,crystallization enthalpy,degree of branching of alkane and thermal stability all show an increasing trend. It can be concluded that solvent extraction coupled with fractional crystallization can obtain refined waxes products with different melting points according to requirements so that the crude waxes with low added value can be better separated.

Keywords:
Fischer-Tropsch waxes
indirect liquefaction
fractional crystallization
narrow fraction
Citation format:
谢浩东(1996—),男,山东安丘人,硕士研究生。E-mail:1356547987@qq.com。通讯作者:陈胜利(1962—),男,教授,博士生导师,博士。E-mail:slchen@cup.edu.cn
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